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2-Chloro-6-nitrobenzaldehyde

  • CasNo:6361-22-4

Product Description

China cas 6361-22-4 factory wholesale 2-Chloro-6-nitrobenzaldehyde at affordable price

  • Molecular Formula: C7H4ClNO3
  • Molecular Weight: 185.567
  • Vapor Pressure: 0.00124mmHg at 25°C 
  • Melting Point: 69-71 °C(lit.) 
  • Refractive Index: 1.63 
  • Boiling Point: 298.8 °C at 760 mmHg 
  • Flash Point: 134.5 °C 
  • PSA： 62.89000 
  • Density: 1.485 g/cm3 
  • LogP: 2.58390 

2-Chloro-6-nitrobenzaldehyde(Cas 6361-22-4) Usage

General Description

2-Chloro-6-nitrobenzaldehyde is a synthetic, organic compound typically used for research and development purposes, particularly in the field of organic chemistry and pharmaceuticals. It is a pale yellow crystalline solid at room temperature and has a moderately complex structure, incorporating elements such as chlorine, nitrogen, a benzene ring, and an aldehyde functional group. Its molecular formula is C7H4ClNO3, and it has a molar mass of 185.57 g/mol. As it is a nitro compound, it has the potential to be explosive under the right conditions and must be handled with care. Its exact properties, such as its boiling and melting points, are dependent on the purity of the substance. Due to its potential hazards, it requires proper storage and handling as per safety guidelines.

InChI:InChI=1/C7H4ClNO3/c8-6-2-1-3-7(9(11)12)5(6)4-10/h1-4H

6361-22-4 Relevant articles

Mild Darzens Annulations for the Assembly of Trifluoromethylthiolated (SCF3) Aziridine and Cyclopropane Structures

Delost, Michael D.,Njardarson, Jon T.

supporting information, p. 6121 - 6125 (2021/08/16)

We report mild new annulation approaches...

METHOD FOR MAKING BIARYL COMPOUNDS, COMPOUNDS MADE BY THE METHOD, AND METHOD FOR THEIR USE

-

Page/Page column 46; 177, (2009/01/23)

Certain disclosed embodiments of the pre...

Diels - Alder approach for the construction of halogenated, o-nitro biaryl templates and application to the total synthesis of the anti-HIV agent siamenol

Naffziger, Michael R.,Ashburn, Bradley O.,Perkins, Johanna R.,Carter, Rich G.

, p. 9857 - 9865 (2008/04/05)

(Chemical Equation Presented) A rapid Di...

Polyaza Heterocycles. Part 2. Nucleophilic Substitution of Halogens in Halogenoquinoxalinocinnolines

Ahmad, Arshad,Dunbar, Linda J.,Green, Iain G.,Harvey, Ian W.,Shepherd, Thomas,et al.

, p. 2751 - 2758 (2007/10/02)

10-Chloroquinoxalinocinnoline readily un...

6361-22-4 Process route

6-chloro-2-nitrotoluene
83-42-1

6-chloro-2-nitrotoluene

<i>N</i>,<i>N</i>-dimethyl-formamide dimethyl acetal
4637-24-5

N ,N -dimethyl-formamide dimethyl acetal

2-chloro-6-nitrobenzaldehyde
6361-22-4

2-chloro-6-nitrobenzaldehyde

Conditions
Conditions Yield
6-chloro-2-nitrotoluene; N,N-dimethyl-formamide dimethyl acetal; In N,N-dimethyl-formamide; at 140 ℃; for 16h;
With sodium periodate; In water; N,N-dimethyl-formamide; at 0 - 20 ℃; for 9h;
86%
6-chloro-2-nitrotoluene
83-42-1

6-chloro-2-nitrotoluene

2-chloro-6-nitrobenzaldehyde
6361-22-4

2-chloro-6-nitrobenzaldehyde

Conditions
Conditions Yield
6-chloro-2-nitrotoluene; With N,N-dimethyl-formamide dimethyl acetal; In N,N-dimethyl-formamide; at 140 ℃; for 16h;
With sodium periodate; In N,N-dimethyl-formamide; at 0 - 20 ℃; Further stages.;
86%
Multi-step reaction with 2 steps
2: 80 percent / 2,2,6,6-tetramethylpiperidine N-oxyl, aq. KBr, NaOCl, NaHCO3 / CH2 Cl2 / 0.5 h / 0 - 5 °C / pH 9.5
With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide; In dichloromethane;
Multi-step reaction with 2 steps
1: bromine / 160 - 180 °C
2: nitric acid
With bromine; nitric acid;
Multi-step reaction with 3 steps
1: NBS, (PhCO)2O2 / CCl4
2: aq. Na2 CO3
3: aq. H2 SO4 , K2 Cr2 O7
With potassium dichromate; N-Bromosuccinimide; sulfuric acid; sodium carbonate; dibenzoyl peroxide; In tetrachloromethane;
6-chloro-2-nitrotoluene; With N,N-dimethyl-formamide dimethyl acetal; In N,N-dimethyl-formamide; at 150 ℃;
In water; N,N-dimethyl-formamide; at 20 ℃;

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